Hydrodynamics and energy consumption studies in a three-phase liquid circulating three-phase fluid bed contactor

The hydrodynamics and energy consumption have been studied in a cold flow, bubbling and turbulent, pressurized gas–liquid–solid three-phase fluidized bed (0.15 m ID × 1 m height) with concurrent gas–liquid up flow is proposed with the intention of increasing the gas hold up. The hydrodynamic behaviour is described and characterised by some specific gas and liquid velocities. Particles are easily fluidized and can be uniformly distributed over the whole height of the column. The effect of parameters like liquid flow rate, gas flow rate, particle loading, particle size, and solid density on gas hold up and effect of gas flow rate, solid density and particle size on solid hold up, energy consumption and minimum fluidization velocity has been studied. At the elevated pressures a superior method for better prediction of minimum fluidization velocity and terminal settling velocities has been adopted. The results have been interpreted with Bernoulli’s theorem and Richardson–Zaki equation. Based on the assumption of the gas and liquid as a pretend fluid, a simplification has been made to predict the particle terminal settling velocities. The Richardson–Zaki parameter n′ was compared with Renzo’s results. A correlation has been proposed with the experimental results for the three-phase fluidization.     

Experimental investigation of slip factors in centrifugal pumps

The phenomenon of slip is known to strongly influence the performance of centrifugal pumps. In the present work, the slip phenomenon at the impeller outlet is studied experimentally for five industrial pumps at different flow rates and the slip factor is estimated for each of these cases. Theoretical slip factors are calculated using several existing methods taking into consideration the main geometric parameters of the impeller. Then the experimental slip factors are compared with the calculated theoretical values.It was observed that in the design-point condition of the pumps, the experimental values are in a good agreement with the theoretical values. However, there are significant disagreements between the theoretical and experimental values at off-design regiments. The difference is more apparent at low flow rates. It is also found that the slip factor depends on the impeller-outlet velocity profile. By defining a flow distortion coefficient, a correlation is derived for evaluating the slip-factor value for off-design conditions.Finally, a slip factor table is provided to calculate the slip factor in centrifugal pumps, using the geometry of impeller.     

One-step Synthesis of 3,4-Dihydrobenzimidazo[2,1- b ]quinazolin-1(2 H )-ones in an Ionic Liquid

A novel class of 3,4-dihydrobenzimidazo[2,1-b]quinazolin-1(2H)-ones was synthesized in very short reaction times with good yields in the presence of 3-butyl-1-methyl imidazolium bromide as a room temperature ionic liquid at 120°C. The ionic liquid can be recycled for subsequent reactions without any loss of efficiency.     

Quantitative Ion-Exchange TLC of p-Hydroxybenzoic Acid in the Presence of Preservatives

JPC – Journal of Planar Chromatography – Modern TLC - Rapid separation of p-hydroxybenzoic acid from methyl p-hydroxy-benzoate, ethyl p-hydroxybenzoate, propyl p-hydroxybenzoate,...     

加权(C)eby(s)ev-Ostrowski型不等式

关于著名的Cebysev不等式，已有众多的研究成果．通过建立积分不等式，来建立全新的加权Cebysev型积分不等式．给予了独立的证明，并给出了此类不等式的新评价．     

A study on the production of PMMA/P(MMA-AAm) composite polymer particles and the effect of acrylamide content on the adsorption behaviors of biomolecules

 A series of poly(methyl methacrylate)/poly(methyl methacrylate-acrylamide) composite polymer particles was prepared with varying proportions of acrylamide in the copolymer shell layer. Adsorption behaviors of some biomolecules and specific activity of adsorbed trypsin were studied. The hydrophobic interaction between the composite polymer particle surfaces and biomolecules decreased with increasing acrylamide content. Received: 7 February 2001 Accepted: 16 May 2001     

Rational design of a BiFeWO6 nanostructure for supercapacitor applications

Journal of Solid State Electrochemistry - Scientists are increasingly interested in improving electroactive technologies for supercapacitor applications, since energy storage devices have improved...     

A validated,rapid and cost-efficient HPTLC method for the quantification of plumbagin and its antioxidant activity from the different extracts of Plumbago zeylanica L.

JPC – Journal of Planar Chromatography – Modern TLC - In the present work, a simple, rapid, reliable and accessible high-performance thin-layer chromatography (HPTLC) technique has been...     

Melting heat transfer in squeezing flow of basefluid (water), nanofluid (CNTs + water) and hybrid nanofluid (CNTs + CuO + water)

Journal of Thermal Analysis and Calorimetry - Unsteady squeezed flow of hybrid nanofluid is investigated in this analysis. Comparison of hybrid nanofluid (using CNTs?+?CuO) and...